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[BMIM]Cl/AlCl_3离子液体低温电沉积铝过程
康艳红; 陈仕谋; 张军玲; 郎海燕; 张锁江
2013
Source Publication化工学报
IssueS1Pages:147-154
Abstract采用玻碳/铂为惰性阳极,以1-丁基-3-甲基咪唑氯盐([BMIM]Cl/AlCl3)离子液体体系为电解液,研究了离子液体电解铝工艺,优化了电解工艺条件,探讨了电解影响因素。结果表明,当电解液[BMIM]Cl∶AlCl3摩尔比为1∶2.00时,随着温度的升高,铝的沉积槽电压逐渐减小,电流密度增加,但电解液的稳定性减弱,当温度达到90℃时,电解液分解明显。当电解温度一定时,随着[BMIM]Cl∶AlCl3摩尔比的增加[(1∶1.25)~(1∶2.00)],电流密度增加。通过赫尔槽实验,SEM、XRD分析了电解铝的沉积形貌和晶相结构。随电流密度的逐渐减小,沉积层变薄,晶相结构变化不大;相同电流密度区随温度的升高,沉积层逐渐变得粗糙。计算了不同槽间距下的槽压与电流密度的关系。
Keyword离子液体 电化学 电解
Document Type期刊论文
Version出版稿
Identifierhttp://ir.ipe.ac.cn/handle/122111/10013
Collection研究所(批量导入)
Recommended Citation
GB/T 7714
康艳红,陈仕谋,张军玲,等. [BMIM]Cl/AlCl_3离子液体低温电沉积铝过程[J]. 化工学报,2013(S1):147-154.
APA 康艳红,陈仕谋,张军玲,郎海燕,&张锁江.(2013).[BMIM]Cl/AlCl_3离子液体低温电沉积铝过程.化工学报(S1),147-154.
MLA 康艳红,et al."[BMIM]Cl/AlCl_3离子液体低温电沉积铝过程".化工学报 .S1(2013):147-154.
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