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5-叔丁基水杨醛的合成与表征
张星; 惠建斌
2011
Source Publication湿法冶金
Issue03Pages:252-254
Abstract无水条件下,以4-叔丁基酚为原料,在甲氧基镁作用下对多聚甲醛进行醛基化反应合成5-叔丁基水杨醛,确立了较优的反应条件:96℃下,n(镁)∶n(4-叔丁基酚):n(多聚甲醛)=1.2∶2∶7,反应时间3 h。最佳条件下,5-叔丁基水杨醛收率达73.1%。采用1HNMR、元素分析对产物进行了结构表征。
Keyword甲氧基镁 醛基化 多聚甲醛 水杨醛 合成 表征
Document Type期刊论文
Version出版稿
Identifierhttp://ir.ipe.ac.cn/handle/122111/10782
Collection研究所(批量导入)
Recommended Citation
GB/T 7714
张星,惠建斌. 5-叔丁基水杨醛的合成与表征[J]. 湿法冶金,2011(03):252-254.
APA 张星,&惠建斌.(2011).5-叔丁基水杨醛的合成与表征.湿法冶金(03),252-254.
MLA 张星,et al."5-叔丁基水杨醛的合成与表征".湿法冶金 .03(2011):252-254.
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