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Large-scale production of well-dispersed submicro ZrB2 and ZrC powders
Bai, Liuyang1,2; Wang, Yongwei1; Chen, Huayi3; Yuan, Fangli1
2016-07-01
发表期刊CRYSTAL RESEARCH AND TECHNOLOGY
ISSN0232-1300
卷号51期号:7页码:428-432
摘要ZrB2 and ZrC powders were synthesized via metallothermic reduction route using ZrO2, B/C, and Mg as raw materials. Low packing density of the green mixture and high heating temperature of the furnace are crucial for the formation of well-dispersed submicro powders. Optimum reaction time helped achieve good crystallization and high purity. The as-prepared samples were characterized by XRD, FESEM, TEM, and particle size analyzer. Results showed that well-dispersed ZrB2 powders with mean particle size of 0.534m and ZrC powders with mean particle size of 0.376m can be obtained. Oxygen content can be controlled lower than 1.0 wt%. The bench-scale output is about 10kg/d.
关键词Borides Carbides Particles Zirconium Zirconium Compounds
文章类型Article
WOS标题词Science & Technology ; Physical Sciences
DOI10.1002/crat.201600051
收录类别SCI
语种英语
关键词[WOS]HIGH-TEMPERATURE CERAMICS ; MECHANICAL-PROPERTIES ; COMPOSITES ; ZIRCONIUM
WOS研究方向Crystallography
WOS类目Crystallography
WOS记录号WOS:000379982900002
引用统计
被引频次:1[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.ipe.ac.cn/handle/122111/21254
专题多相复杂系统国家重点实验室
作者单位1.Chinese Acad Sci, State Key Lab Multiphase Complex Syst, Inst Proc Engn, Beijing 100190, Peoples R China
2.Hebei Normal Univ Nationalities, Dept Chem, Chengde 067000, Peoples R China
3.China Pingmei Shenma Grp Engn Plast Co Ltd, Pingdingshan 467000, Peoples R China
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GB/T 7714
Bai, Liuyang,Wang, Yongwei,Chen, Huayi,et al. Large-scale production of well-dispersed submicro ZrB2 and ZrC powders[J]. CRYSTAL RESEARCH AND TECHNOLOGY,2016,51(7):428-432.
APA Bai, Liuyang,Wang, Yongwei,Chen, Huayi,&Yuan, Fangli.(2016).Large-scale production of well-dispersed submicro ZrB2 and ZrC powders.CRYSTAL RESEARCH AND TECHNOLOGY,51(7),428-432.
MLA Bai, Liuyang,et al."Large-scale production of well-dispersed submicro ZrB2 and ZrC powders".CRYSTAL RESEARCH AND TECHNOLOGY 51.7(2016):428-432.
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