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Preparation of Anhydrous Magnesium Chloride from Ammonium Carnallite
Zhang, Zhimin1,2; Lu, Xuchen1,3; Yang, Suping1,2; Pan, Feng1,2; Wang, Yun1,2; Lu, XC
2012
发表期刊MATERIALS AND MANUFACTURING PROCESSES
ISSN1042-6914
卷号28期号:1页码:5-9
摘要High-purity anhydrous magnesium chloride was prepared by using ammonium carnallite as starting material and alumina as covering agent. X-ray diffraction (XRD) analysis and thermogravimetric analysis and differential calorimetry analysis (TG-DSC) analysis were employed to characterize the process. The mechanism involved in the process was proposed and discussed. The factors affecting the purity of anhydrous magnesium chloride were investigated. The results reveal that the mass fraction of magnesia in anhydrous magnesium chloride could reach 0.08% under the optimum conditions: alumina with the thickness of 1.3 cm was put on top of dehydrated ammonium chloride (NH4Cl center dot MgCl2 center dot 1.2H(2)O), and then the sample was maintained at 450 degrees C for 1.5 h. After that, the sample was calcined at 700 degrees C for 1 h.
关键词Characterization Electrochemical Electrochemistry Engineering Magnesium Sintering Synthesis
文章类型Article
WOS标题词Science & Technology ; Technology
DOI10.1080/10426914.2012.718479
收录类别SCI
语种英语
关键词[WOS]THERMAL-DECOMPOSITION ; ALLOY ; ZK60
WOS研究方向Engineering ; Materials Science
WOS类目Engineering, Manufacturing ; Materials Science, Multidisciplinary
WOS记录号WOS:000313416700002
引用统计
被引频次:1[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
版本出版稿
条目标识符http://ir.ipe.ac.cn/handle/122111/2678
专题多相复杂系统国家重点实验室
通讯作者Lu, XC
作者单位1.Chinese Acad Sci, Inst Proc Engn, State Key Lab Multiphase Complex Syst, Beijing, Peoples R China
2.Chinese Acad Sci, Grad Univ, Beijing, Peoples R China
3.United Res Ctr Resource & Mat, Wuhai, Peoples R China
推荐引用方式
GB/T 7714
Zhang, Zhimin,Lu, Xuchen,Yang, Suping,et al. Preparation of Anhydrous Magnesium Chloride from Ammonium Carnallite[J]. MATERIALS AND MANUFACTURING PROCESSES,2012,28(1):5-9.
APA Zhang, Zhimin,Lu, Xuchen,Yang, Suping,Pan, Feng,Wang, Yun,&Lu, XC.(2012).Preparation of Anhydrous Magnesium Chloride from Ammonium Carnallite.MATERIALS AND MANUFACTURING PROCESSES,28(1),5-9.
MLA Zhang, Zhimin,et al."Preparation of Anhydrous Magnesium Chloride from Ammonium Carnallite".MATERIALS AND MANUFACTURING PROCESSES 28.1(2012):5-9.
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