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Hydrothermal synthesis of boehmites with various particle sizes and transition to α-Al2O3 powders by calcination | |
Hu P(胡鹏)![]() ![]() ![]() | |
2005 | |
Source Publication | 广东有色金属学报
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ISSN | 1003-7837 |
Volume | 15.0Issue:002Pages:581 |
Abstract | Boehmite powders with various particle sizes have becn prepared by hydrothermal method and the α-Al2O3 powders yieldcd after subsequent calcination have been studied, Dispersive crystalline boehmite powders of 30-100 nm, 0, 4-0, 6μm and 1μm in size were obtained respectively by changing the hydrothermal precursors and the pH value of hydrothermal slurry. Calcination of boehmite powders of 30-100 nm at 1250℃ for lh resulted in the formation of single phase α-Al2O3, and the products consisted of vermicular particles. The boehmite powders of 0.4-0, 6μm were also fully converted to α-Al2O3 at 1250℃, and the products consisted of plate-like particles with the same size of 0, 4-0, 6μm, The boehmite powders of 1μm calcined at 1350℃ for 2h were still composed of a little proportions of transition aluminas besides α-Al2O3, and the particles sitiered severely. The reaction processes for the formation of crystalline boehmites under hydrothermal conditions and α-Al2O3 powders during calcination have been discussed. |
Keyword | 热液合成 一水软铝石 粒子结构 粉末 结构材料 |
Language | 英语 |
Document Type | 期刊论文 |
Identifier | http://ir.ipe.ac.cn/handle/122111/47303 |
Collection | 中国科学院过程工程研究所 |
Affiliation | 中国科学院过程工程研究所 |
First Author Affilication | 中国科学院过程工程研究所 |
Recommended Citation GB/T 7714 | Hu P,Hu P,Hu P. Hydrothermal synthesis of boehmites with various particle sizes and transition to α-Al2O3 powders by calcination[J]. 广东有色金属学报,2005,15.0(002):581. |
APA | 胡鹏,胡鹏,&胡鹏.(2005).Hydrothermal synthesis of boehmites with various particle sizes and transition to α-Al2O3 powders by calcination.广东有色金属学报,15.0(002),581. |
MLA | 胡鹏,et al."Hydrothermal synthesis of boehmites with various particle sizes and transition to α-Al2O3 powders by calcination".广东有色金属学报 15.0.002(2005):581. |
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