CAS OpenIR
Molten salt synthesis of TiB2 nanopowder by reduction of TiO2 with MgB2
Shah, Liaqat Ali
2021
Source PublicationPROCESSING AND APPLICATION OF CERAMICS
ISSN1820-6131
Volume15Issue:1Pages:8
AbstractThis research work presents the preparation of TiB2 nanopowders by molten-salt synthesis (MSS) technique from TiO2 and MgB2 as starting active materials and MgCl2 as a molten salt. The pure TiB2 nanopowders were finally prepared using 2 M HCl aqueous solution to leach the synthesized samples. The effects of the firing temperature, firing time and reactants to salt ratio on the TiB2 nanopowders formation were examined. The results demonstrated that the TiB2 formation was completed even with reactants to salt mass ratio of 1:2 at 1000 degrees C for 4 h. The TiB2 nanopowders synthesized with 1:2, 1:5 and 1:10 reactants to salt mass ratios have different particle sizes. Thus, the average particle sizes estimated from BET surface areas were 59, 55 and 46 nm for the samples synthesized with 1: 2, 1:5 and 1:10 reactants to salts mass ratios, respectively. These results illustrated that the high concentration of MgCl2 plays a key role in the particles' size reduction. The above results assured that this research study presents a new low-temperature synthesis rout for nanosized metal diboride powders.
Keywordmolten salt synthesis low temperature surface area TiB2 particle size
Language英语
Funding ProjectChinese Academy of Sciences[2017PE0006]
WOS Research AreaMaterials Science
WOS SubjectMaterials Science, Ceramics
Funding OrganizationChinese Academy of Sciences
WOS IDWOS:000636430700001
PublisherUNIV NOVI SAD, FAC TECHNOLOGY
Citation statistics
Cited Times:1[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.ipe.ac.cn/handle/122111/48202
Collection中国科学院过程工程研究所
Corresponding AuthorShah, Liaqat Ali
AffiliationChinese Acad Sci, Inst Proc Engn, State Key Lab Multiphase Complex Syst, Beijing, Peoples R China
Recommended Citation
GB/T 7714
Shah, Liaqat Ali. Molten salt synthesis of TiB2 nanopowder by reduction of TiO2 with MgB2[J]. PROCESSING AND APPLICATION OF CERAMICS,2021,15(1):8.
APA Shah, Liaqat Ali.(2021).Molten salt synthesis of TiB2 nanopowder by reduction of TiO2 with MgB2.PROCESSING AND APPLICATION OF CERAMICS,15(1),8.
MLA Shah, Liaqat Ali."Molten salt synthesis of TiB2 nanopowder by reduction of TiO2 with MgB2".PROCESSING AND APPLICATION OF CERAMICS 15.1(2021):8.
Files in This Item:
There are no files associated with this item.
Related Services
Recommend this item
Bookmark
Usage statistics
Export to Endnote
Google Scholar
Similar articles in Google Scholar
[Shah, Liaqat Ali]'s Articles
Baidu academic
Similar articles in Baidu academic
[Shah, Liaqat Ali]'s Articles
Bing Scholar
Similar articles in Bing Scholar
[Shah, Liaqat Ali]'s Articles
Terms of Use
No data!
Social Bookmark/Share
All comments (0)
No comment.
 

Items in the repository are protected by copyright, with all rights reserved, unless otherwise indicated.