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An investigation on the oxidation behavior of spatters generated during the laser powder bed fusion of 316L stainless steel
Lu, Chao1; Zhang, Ruihua1,2; Wei, Xiaohong2; Xiao, Mengzhi1; Yin, Yan3; Qu, Yuebo1; Li, Hui1; Liu, Pengyu1; Qiu, Xiaopan4; Guo, Tieming3
2022-06-01
Source PublicationAPPLIED SURFACE SCIENCE
ISSN0169-4332
Volume586Pages:17
AbstractThe characterization of the oxide islands on the surface of the spatter contributes to a fundamental understanding of the formation and oxidation of spatter in laser powder bed fusion (LPBF). In the present study, the surface and cross-section characteristics of spatters with oxide islands are investigated using high resolution scanning electron microscopy combined with energy dispersive spectroscopy, scanning transmission electron microscopy and selected area electron diffraction. The oxide islands with different configurations on the spatter surface are divided into three main categories: hemispherical, disc-like and film-like. Moreover, the primary component of oxide islands is an amorphous SiO2, which may also contain MnO, MnSiO3, and Mn2SiO4. Furthermore, a transition layer (enriched in Si, Mn, and O) is found at the oxide islands || spatter substrate interface, and the width of which is 4 mu m and 20 nm on the spatter surface and within the spatter cross-section, respectively. Besides, the composition and sources of the circular oxide nano-inclusions (50-600 nm) internal to the spatters are also discussed in detail. Eventually, the driving forces affecting the formation of oxide islands on the surface of spatters are summarized, and a schematic diagram of the formation procedure is developed.
KeywordLaser powder bed fusion Spatter Oxidation behavior Oxide islands Surface characterization
DOI10.1016/j.apsusc.2022.152796
Language英语
WOS KeywordNI-BASED NANOCOMPOSITES ; HIGH-STRENGTH ; METALLIC COMPONENTS ; GAS ATOMIZATION ; SURFACE ; MICROSTRUCTURE ; ION ; DENSIFICATION ; DENUDATION ; MECHANISMS
Funding ProjectYangjiang City Science and Technology Plan Project[2018057] ; Yangjiang City Science and Technology Plan Project[SDZX2019038] ; Yangjiang City Science and Technology Plan Project[SDZX2020009] ; Yangjiang City Science and Technology Plan Project[2018002] ; National Natural Science Foundation of China[52161007]
WOS Research AreaChemistry ; Materials Science ; Physics
WOS SubjectChemistry, Physical ; Materials Science, Coatings & Films ; Physics, Applied ; Physics, Condensed Matter
Funding OrganizationYangjiang City Science and Technology Plan Project ; National Natural Science Foundation of China
WOS IDWOS:000775635500001
PublisherELSEVIER
Citation statistics
Document Type期刊论文
Identifierhttp://ir.ipe.ac.cn/handle/122111/52609
Collection中国科学院过程工程研究所
Corresponding AuthorLu, Chao; Zhang, Ruihua
Affiliation1.Cent Iron & Steel Res Inst, Beijing 100081, Peoples R China
2.Hardware Knife Cut Ind Technol Res Inst Yangjiang, Yangjiang 529533, Peoples R China
3.Lanzhou Univ Technol, Sch Mat Sci & Engn, Lanzhou 730050, Peoples R China
4.Chinese Acad Sci, Inst Proc Engn, State Key Lab Multiphase Complex Syst, Beijing 100190, Peoples R China
Recommended Citation
GB/T 7714
Lu, Chao,Zhang, Ruihua,Wei, Xiaohong,et al. An investigation on the oxidation behavior of spatters generated during the laser powder bed fusion of 316L stainless steel[J]. APPLIED SURFACE SCIENCE,2022,586:17.
APA Lu, Chao.,Zhang, Ruihua.,Wei, Xiaohong.,Xiao, Mengzhi.,Yin, Yan.,...&Guo, Tieming.(2022).An investigation on the oxidation behavior of spatters generated during the laser powder bed fusion of 316L stainless steel.APPLIED SURFACE SCIENCE,586,17.
MLA Lu, Chao,et al."An investigation on the oxidation behavior of spatters generated during the laser powder bed fusion of 316L stainless steel".APPLIED SURFACE SCIENCE 586(2022):17.
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