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An investigation on the oxidation behavior of spatters generated during the laser powder bed fusion of 316L stainless steel | |
Lu, Chao1; Zhang, Ruihua1,2; Wei, Xiaohong2; Xiao, Mengzhi1; Yin, Yan3; Qu, Yuebo1; Li, Hui1; Liu, Pengyu1; Qiu, Xiaopan4; Guo, Tieming3 | |
2022-06-01 | |
Source Publication | APPLIED SURFACE SCIENCE
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ISSN | 0169-4332 |
Volume | 586Pages:17 |
Abstract | The characterization of the oxide islands on the surface of the spatter contributes to a fundamental understanding of the formation and oxidation of spatter in laser powder bed fusion (LPBF). In the present study, the surface and cross-section characteristics of spatters with oxide islands are investigated using high resolution scanning electron microscopy combined with energy dispersive spectroscopy, scanning transmission electron microscopy and selected area electron diffraction. The oxide islands with different configurations on the spatter surface are divided into three main categories: hemispherical, disc-like and film-like. Moreover, the primary component of oxide islands is an amorphous SiO2, which may also contain MnO, MnSiO3, and Mn2SiO4. Furthermore, a transition layer (enriched in Si, Mn, and O) is found at the oxide islands || spatter substrate interface, and the width of which is 4 mu m and 20 nm on the spatter surface and within the spatter cross-section, respectively. Besides, the composition and sources of the circular oxide nano-inclusions (50-600 nm) internal to the spatters are also discussed in detail. Eventually, the driving forces affecting the formation of oxide islands on the surface of spatters are summarized, and a schematic diagram of the formation procedure is developed. |
Keyword | Laser powder bed fusion Spatter Oxidation behavior Oxide islands Surface characterization |
DOI | 10.1016/j.apsusc.2022.152796 |
Language | 英语 |
WOS Keyword | NI-BASED NANOCOMPOSITES ; HIGH-STRENGTH ; METALLIC COMPONENTS ; GAS ATOMIZATION ; SURFACE ; MICROSTRUCTURE ; ION ; DENSIFICATION ; DENUDATION ; MECHANISMS |
Funding Project | Yangjiang City Science and Technology Plan Project[2018057] ; Yangjiang City Science and Technology Plan Project[SDZX2019038] ; Yangjiang City Science and Technology Plan Project[SDZX2020009] ; Yangjiang City Science and Technology Plan Project[2018002] ; National Natural Science Foundation of China[52161007] |
WOS Research Area | Chemistry ; Materials Science ; Physics |
WOS Subject | Chemistry, Physical ; Materials Science, Coatings & Films ; Physics, Applied ; Physics, Condensed Matter |
Funding Organization | Yangjiang City Science and Technology Plan Project ; National Natural Science Foundation of China |
WOS ID | WOS:000775635500001 |
Publisher | ELSEVIER |
Citation statistics | |
Document Type | 期刊论文 |
Identifier | http://ir.ipe.ac.cn/handle/122111/52609 |
Collection | 中国科学院过程工程研究所 |
Corresponding Author | Lu, Chao; Zhang, Ruihua |
Affiliation | 1.Cent Iron & Steel Res Inst, Beijing 100081, Peoples R China 2.Hardware Knife Cut Ind Technol Res Inst Yangjiang, Yangjiang 529533, Peoples R China 3.Lanzhou Univ Technol, Sch Mat Sci & Engn, Lanzhou 730050, Peoples R China 4.Chinese Acad Sci, Inst Proc Engn, State Key Lab Multiphase Complex Syst, Beijing 100190, Peoples R China |
Recommended Citation GB/T 7714 | Lu, Chao,Zhang, Ruihua,Wei, Xiaohong,et al. An investigation on the oxidation behavior of spatters generated during the laser powder bed fusion of 316L stainless steel[J]. APPLIED SURFACE SCIENCE,2022,586:17. |
APA | Lu, Chao.,Zhang, Ruihua.,Wei, Xiaohong.,Xiao, Mengzhi.,Yin, Yan.,...&Guo, Tieming.(2022).An investigation on the oxidation behavior of spatters generated during the laser powder bed fusion of 316L stainless steel.APPLIED SURFACE SCIENCE,586,17. |
MLA | Lu, Chao,et al."An investigation on the oxidation behavior of spatters generated during the laser powder bed fusion of 316L stainless steel".APPLIED SURFACE SCIENCE 586(2022):17. |
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