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Preparation and characterization of ultrafine ZrO2 powders from solvent extraction of Zr(IV) with tri-n-butyl phosphate in kerosene from nitric acid solutions
Alternative TitleJ. Mater. Sci. Technol.
Yang, CF; Chen, JY
1996-12-01
Source PublicationJOURNAL OF MATERIALS SCIENCE & TECHNOLOGY
ISSN1005-0302
Volume12Issue:6Pages:439-444
AbstractZr(IV) was extracted by tri-n-butyl phosphate in kerosene from concentrated nitric acid solutions and the formation of the third phase during extraction was experimentally investigated. Zirconia powders were prepared by using the loaded organic phase as the bulk solution precipitated with aqueous ammonia or NaOH solution. The powder prepared was characterized with TEM, XRD, EDAX and TG-DTA. Effects of some conditions on powder preparation were studied and it was shown that nanosized particles could be obtained from this extraction system but conditions should be carefully controlled for powder purity and particle size.; Zr(IV) was extracted by tri-n-butyl phosphate in kerosene from concentrated nitric acid solutions and the formation of the third phase during extraction was experimentally investigated. Zirconia powders were prepared by using the loaded organic phase as the bulk solution precipitated with aqueous ammonia or NaOH solution. The powder prepared was characterized with TEM, XRD, EDAX and TG-DTA. Effects of some conditions on powder preparation were studied and it was shown that nanosized particles could be obtained from this extraction system but conditions should be carefully controlled for powder purity and particle size.
KeywordMicroemulsions Particles System Micelles
SubtypeArticle
WOS HeadingsScience & Technology ; Technology
URL查看原文
Indexed BySCI
Language英语
WOS KeywordMICROEMULSIONS ; PARTICLES ; SYSTEM ; MICELLES
WOS Research AreaMaterials Science ; Metallurgy & Metallurgical Engineering
WOS SubjectMaterials Science, Multidisciplinary ; Metallurgy & Metallurgical Engineering
WOS IDWOS:A1996WD93400008
Citation statistics
Cited Times:5[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Version出版稿
Identifierhttp://ir.ipe.ac.cn/handle/122111/6024
Collection研究所(批量导入)
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GB/T 7714
Yang, CF,Chen, JY. Preparation and characterization of ultrafine ZrO2 powders from solvent extraction of Zr(IV) with tri-n-butyl phosphate in kerosene from nitric acid solutions[J]. JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY,1996,12(6):439-444.
APA Yang, CF,&Chen, JY.(1996).Preparation and characterization of ultrafine ZrO2 powders from solvent extraction of Zr(IV) with tri-n-butyl phosphate in kerosene from nitric acid solutions.JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY,12(6),439-444.
MLA Yang, CF,et al."Preparation and characterization of ultrafine ZrO2 powders from solvent extraction of Zr(IV) with tri-n-butyl phosphate in kerosene from nitric acid solutions".JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY 12.6(1996):439-444.
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