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手性HPLC法测定布洛芬立体选择性酯化的转化率和对映体过量
谢渝春; 刘会洲; 陈家镛
1998
Source Publication色谱
Issue01Pages:58-60
Abstract以脂肪酶在正己烷中催化消旋布洛芬与正丁醇的立体选择性酯化反应为例,研究了用手性HPLC法进行分析时产物及底物的峰面积变化与转化率的关系,确定了布洛芬丁酯与未反应布洛芬的峰面积-浓度响应因子的比值,从而可通过一次进样用峰面积直接测定布洛芬的转化率和对映体过量。
Keyword手性高效液相色谱法 布洛芬 转化率 对映体过量
Document Type期刊论文
Version出版稿
Identifierhttp://ir.ipe.ac.cn/handle/122111/7526
Collection研究所(批量导入)
Recommended Citation
GB/T 7714
谢渝春,刘会洲,陈家镛. 手性HPLC法测定布洛芬立体选择性酯化的转化率和对映体过量[J]. 色谱,1998(01):58-60.
APA 谢渝春,刘会洲,&陈家镛.(1998).手性HPLC法测定布洛芬立体选择性酯化的转化率和对映体过量.色谱(01),58-60.
MLA 谢渝春,et al."手性HPLC法测定布洛芬立体选择性酯化的转化率和对映体过量".色谱 .01(1998):58-60.
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