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4,4′-MDC与其分解产物4,4′-MDI的高效液相色谱分析
关雪; 李会泉; 郭奋; 裴义霞; 柳海涛; 姚星星
2009
Source Publication化学试剂
Issue10Pages:807-808+830
Abstract针对4,4′-二苯甲烷二氨基甲酸甲酯(4,4′-MDC)分解制备4,4′-二苯甲烷二异氰酸酯(4,4′-MDI)的反应过程,利用高效液相色谱分析方法同时实现原料及产品的定量分析。采用二正丁胺为封端衍生剂,封端反应结束后采用甲醇为溶剂稀释,确定了最佳分析条件。该方法快速简便,精密度、准确度都较高,适于该反应的定量分析,取得了较满意的结果。
Keyword二苯甲烷二氨基甲酸甲酯 二苯甲烷二异氰酸酯 高效液相色谱
Document Type期刊论文
Identifierhttp://ir.ipe.ac.cn/handle/122111/9913
Collection研究所(批量导入)
Recommended Citation
GB/T 7714
关雪,李会泉,郭奋,等. 4,4′-MDC与其分解产物4,4′-MDI的高效液相色谱分析[J]. 化学试剂,2009(10):807-808+830.
APA 关雪,李会泉,郭奋,裴义霞,柳海涛,&姚星星.(2009).4,4′-MDC与其分解产物4,4′-MDI的高效液相色谱分析.化学试剂(10),807-808+830.
MLA 关雪,et al."4,4′-MDC与其分解产物4,4′-MDI的高效液相色谱分析".化学试剂 .10(2009):807-808+830.
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